HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromomethylcyclopropane → HCID 66818544, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromomethylcyclopropane | HCID 81503 | — |
| Reactant | HCID 66818471 | HCID 66818471 | — |
| Product | HCID 66818544 | HCID 66818544 | 59.4% |
Reaction Steps
Following the procedure of Example 11(e) 4-[3,5-bis-(4-cyano-phenoxy)-phenyl-carbamoyl]-piperidine 1.5 g (3.42 mmol) and bromomethylcyclopropane (0.647 g, 4.79 mmol) were used to afford 1.0 g of the required product. Percentage purity (LCMS): 73.1%, (M+1)=492.1+1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08722930B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-a304da056b774a76a256c5273b1a4768 |
| Source note | uspto-grants-2014_05 |