HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromomethylcyclopropane → HCID 66818748, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromomethylcyclopropane | HCID 81503 | — |
| Reactant | HCID 66818786 | HCID 66818786 | — |
| Product | HCID 66818748 | HCID 66818748 | 71.2% |
Reaction Steps
Following procedure of Example 11(e) 3,5-bis-(4-cyano-phenoxy)-N-piperidin-4-yl-benzamide 0.5 g (1.14 mmol) and bromomethyl-cyclopropane (0.231 g, 1.71 mmol) were used to afford 0.4 g of the required product. Percentage purity (LCMS): 45.0%, (M+1)=492.2+1
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08722930B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-1824fed9f4024f3c8fb5017ee3a0711f |
| Source note | uspto-grants-2014_05 |