HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfamide → 4-Pyrimidin-2-ylpiperazine-1-sulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfamide | HCID 82267 | — |
| Reactant | 1-(2-Pyrimidinyl)piperazine | HCID 88747 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | 4-Pyrimidin-2-ylpiperazine-1-sulfonamide | HCID 11572297 | — |
Reaction Steps
The subtitle compound was prepared according to the procedure outlined in example 15 step i) using 2-piperazin-1-ylpyrimidine (3.0 g) and sulfamide (1.2 g) in dioxane (30 mL) to give the subtitle compound as a white solid. Yield: 2.06 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08722883B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-8da0ba42c50043f8ba9b3790f6910dfe |
| Source note | uspto-grants-2014_05 |