反应详情

To a solution of 0.88 NH3 (50 ml) was added benzyl 4-(chlorosulfonyl)piperidine-1-carboxylate (4 g) and the reaction stirred for 72 h at RT. The reaction was then extracted with DCM (3×150 ml). Organics were recovered, dried (MgSO4) and reduced in vacuo to give the subtitle compound as a clear oil. Yield 3.3 g

1. extractionThe reaction was then extracted with DCM (3×150 ml)
2. customOrganics were recovered
3. dry with materialdried (MgSO4)