HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formaldehyde → 2,3-Dimethylbenzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formaldehyde | HCID 712 | — |
| Reactant | Phenol | HCID 996 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | M-Xylene | HCID 7929 | — |
| Product | 2,3-Dimethylbenzaldehyde | HCID 34224 | — |
Reaction Steps
A 2-liter flask equipped with a thermometer, a reflux condenser, and a stirrer was charged with 480 parts of 50% formalin, 110 parts of phenol, 202 parts of 98% industrial sulfuric acid, and 424 parts of m-xylene. The resulting mixture was allowed to react at 84 to 88° C. for 4 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08728626B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-6deac67a02814a23a2efec3649b50da9 |
| Source note | uspto-grants-2014_05 |