HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium periodate → HCID 24829985, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium periodate | HCID 23667635 | — |
| Reactant | HCID 24829988 | HCID 24829988 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 24829985 | HCID 24829985 | — |
Reaction Steps
A solution of Compound 9 was dissolved in 2:1 isopropyl alcohol and water and stirred at room temp. Sodium periodate (1 eq.) was added and the reaction was stirred overnight, quenched with water and washed with ethyl acetate. The organic layer was dried and concentrated to yield 38.0 mg Compound 6.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08729069B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-9b452558162843a296d925e788309ce8 |
| Source note | uspto-grants-2014_05 |