huagongshe.com
HRID1025844

反应详情

EQUATION

反应方程式

HRID 1025844 的结构方程式

REACTANTS

反应物

2
结构：CCCCCCC.CCOC(C)=O
HCID21899848

未命名化合物

结构：CN(C)c1ncccc1NC(=O)c1cnccc1Oc1cc(Cl)ccc1Cl
HCID67320131

未命名化合物

PRODUCTS

生成物

1
结构：CN(C)c1ncccc1N(C)C(=O)c1cnccc1Oc1cc(Cl)ccc1Cl
HCID53312108

未命名化合物

PROCEDURE

实验过程

The title compound was prepared in analogy to Example 12, from 4-(2,5-dichloro-phenoxy)-N-(2-dimethylamino-pyridin-3-yl)-nicotinamide and using a gradient of n-heptane:ethyl acetate (100:0 to 0:100) for the chromatographic purification. Colorless oil (67%). MS (ESI): m/z=417.088 [M+H]+.

WORKUP

后处理

  1. customfor the chromatographic purification