Acetyl chloride → HCID 24937926, compound

Participants

Reaction Steps

To a solution of N′1,N′3-dimethyl-N′1,N′3-di(phenylcarbonothioyl)malonohydrazide (a, 2.0 mmol) in TEA (5 mL) and DCM (10 mL) was added dropwise acetyl chloride (4.0 mmol) and the mixture was stirred at rt for 12 h before quenching with aqueous 1N NaHCO3 (10 mL). The organic layer was separated and evaporated. The residue was purified by flash chromatography to give b as yellow solids (7 mg).

Provenance & Evidence