HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl Sulfide → HCID 68698175, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl Sulfide | HCID 1068 | — |
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | HCID 68700839 | HCID 68700839 | — |
| Catalyst | Zincchloride | HCID 3007855 | — |
| Product | HCID 68698175 | HCID 68698175 | 65% |
Reaction Steps
The compound was prepared by reacting (S)-{3-[4-(4,4-dimethoxy-3-fluoropiperidin-1-yl)-phenyl]-2-oxo-oxazolidin-5-ylmethyl}-acetamide with zinc chloride, dimethyl sulphide and acetyl chloride as per procedure described in Example E in 65% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08729269B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-ef4b66420ca847798baa8977da1b147a |
| Source note | uspto-grants-2014_05 |