HRID1026658

反应详情

EQUATION

反应方程式

HRID 1026658 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

The title compound was prepared by stirring (S)—N-{3-[4-(4-methyl-4-hydroxy piperidin-1-yl)-3-fluorophenyl]-2-oxo-oxazolidin-5-ylmethyl}-acetamide (1.36 mmol) with DAST (1.64 mmol) in dichloromethane (10 ml) at a temperature 0° C. for half hour and by purifying the compound by silica gel column chromatography in 66% yield.

WORKUP

后处理

  1. customby purifying the compound by silica gel column chromatography in 66% yield