HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 11463102, compound → HCID 11373155, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 11463102 | HCID 11463102 | — |
| Reactant | Methanol--water (1/1) | HCID 22242641 | — |
| Reactant | Sodium periodate | HCID 23667635 | — |
| Product | HCID 11373155 | HCID 11373155 | 57% |
Reaction Steps
The title compound was prepared by reacting (S)—N-{3-[4-(1-thia-6-aza-spiro[2.5]oct-6-yl)-3-fluorophenyl]-2-oxo-oxazolidin-5-ylmethyl}-acetamide (0.4 mmol) and sodium periodate (mmol) in methanol water mixture (10 ml) at a temperature 25-30° C. for 14 hours in 57% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08729269B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-ae1853cb3f9648e5a71dfa41652f29b9 |
| Source note | uspto-grants-2014_05 |