HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylene Glycol → HCID 59754073, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylene Glycol | HCID 174 | — |
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Reactant | HCID 59754123 | HCID 59754123 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 59754073 | HCID 59754073 | 69% |
Reaction Steps
The compound was prepared by reacting (S)—N-{3-[4-(4-oxo-piperidin-1-yl)-phenyl]-2-oxo-oxazolidin-5-ylmethyl}-acetamide (0.5 mmol), ethylene glycol (0.5 mmol), p-toluene sulfonic acid (0.3 mmol) in toluene and by purifying on silica gel column chromatography to provide title compound in 69% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08729269B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-17a55a4ef66c424c909bdca2eb32d813 |
| Source note | uspto-grants-2014_05 |