Hexane → 1-(4-bromophenyl)naphthalene

HRID 1026788Notes

Reaction equation

HRID 1026788 reaction equation
[Br:1][C:2]1[CH:7]=[CH:6][C:5](I)=[CH:4][CH:3]=1.[CH3:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14]>>[Br:1][C:2]1[CH:7]=[CH:6][C:5]([C:11]2[C:10]3[C:7](=[CH:2][CH:3]=[CH:4][CH:9]=3)[CH:14]=[CH:13][CH:12]=2)=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 8058HexaneHCID 115221-Bromo-4-iodobenzene

Product 1

HCID 112083381-(4-bromophenyl)naphthalene

Procedure

An Rf value of the desired substance by a silica gel thin layer chromatography (TLC) (developing solvent: hexane) was 0.38 and that of 4-bromoiodobenzene was 0.57.

Sources & evidence

ORD record
ord-8c6b48255581494aacb0c235dd09a933
Source dataset
uspto-grants-2014_05
Patent number
US08729310B2

Reaction notes

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