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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1027520Generated: October 30, 2026

3-Phenyl-allyldisulfanyl-3-allylbenzene → HCID 178435948, compound

https://huagongshe.com/reaction/1027520

Reaction equation

Participants

RoleNameHCIDCharge
Reactant3-Phenyl-allyldisulfanyl-3-allylbenzeneHCID 86712988—
ReactantHCID 178419464HCID 178419464—
ReactantHCID 178503312HCID 178503312—
SolventEthyl AcetateHCID 8857—
ProductHCID 178435948HCID 17843594822%

Reaction Steps

Compound 21K was prepared following the procedure as described for the synthesis of compound 21A (see Scheme 3) using 3-phenyl-allyldisulfanyl-3-allylbenzene as the disulfide (Tetrahedron Letters, 42, 2001, 6741-6743) and 3-(4-bromo-1H-pyrazol-3-yl)-pyridine (compound 20A). (conditions flash chromatography (ethyl acetate)). Yield: 22%. (oil), (TLC ethyl acetate Rf 0.45).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08735388B2
Source datasetuspto-grants-2014_05
ORD IDord-595726a8e55c4f87bbaf06ea69795abb
Source noteuspto-grants-2014_05