HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(1-phenylsulfonyl-4-hex-1-ynyl-1H-pyrazol-3-yl)-pyridine → HCID 178437212, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(1-phenylsulfonyl-4-hex-1-ynyl-1H-pyrazol-3-yl)-pyridine | HCID 57548044 | — |
| Reactant | 3-[1-phenylsulfonyl-4-(5-phenyl-pent-1-ynyl)-1H-pyrazol-3-yl]-pyridine | HCID 67284086 | — |
| Reactant | 3-(4-Hex-1-ynyl-1H-pyrazol-3-yl)-1,2,5,6-tetrahydro-1-methylpyridine | HCID 178442470 | — |
| Product | HCID 178437212 | HCID 178437212 | — |
Reaction Steps
Compound 43D was converted to the title compound 44D, using the methodology described for the conversion of 43A to 44A (see Scheme 9). Yield: 86% (oil). 1H-NMR (400 MHz, CDCl3): δ 9.25 (d, J=2 Hz, 1H), 8.6 (dd, J=5 Hz, 2 Hz, 1H), 8.35 (dt, J=8 Hz, 2 Hz, 1H), 7.74 (s, 1H), 7.40-7.17 (m, 6H), 2.77 ((t, J=7 Hz, 2H), 2.44 ((t, J=7 Hz, 2H), 1.99-1.89 (m, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08735388B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-ae59cff288454fb1b19baed3b82c76cf |
| Source note | uspto-grants-2014_05 |