Ethanethiol → HCID 178477307, compound

HRID 1027547Notes

Reaction equation

HRID 1027547 reaction equation
[CH2:1]([S:6][C:7]1[C:8]([CH:12]2[CH:17]3[CH2:18][CH2:19][N:14]([CH2:15][CH2:16]3)[CH2:13]2)=[N:9][NH:10][CH:11]=1)[CH2:2]CCC.C(S)C>>[CH2:1]([S:6][C:7]1[C:8]([CH:12]2[CH:17]3[CH2:16][CH2:15][N:14]([CH2:19][CH2:18]3)[CH2:13]2)=[N:9][NH:10][CH:11]=1)[CH3:2]

Participants

3

Reactant 2

HCID 6343EthanethiolHCID 178447695HCID 178447695, compound

Product 1

HCID 178477307HCID 178477307, compoundYield 30%

Procedure

Compound 49D was prepared following the procedure as described for the synthesis of compound 49B (see Scheme 10) using ethanethiol as reagent. Subsequent purification by flash chromatography (EtOH to EtOH/triethylamine 99/1) afforded compound 49D.

Workup

  1. customSubsequent purification by flash chromatography (EtOH to EtOH/triethylamine 99/1)

Sources & evidence

ORD record
ord-72955bd6932947a594ed7350bf51dba4
Source dataset
uspto-grants-2014_05
Patent number
US08735388B2

Reaction notes

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