HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → 3-Methoxy-2-nitropyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 3-Hydroxy-2-nitropyridine | HCID 27057 | — |
| Product | 3-Methoxy-2-nitropyridine | HCID 556063 | 97.4% |
Reaction Steps
The similar reaction as described in Reference Example 9 by using 2-nitro-3-hydroxypyridine (7.0 g), potassium carbonate (6.91 g) and methyl iodide (4.67 ml) gave the title compound (7.5 g) as crystalline powders.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08735401B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-33681630cd1e4562bb0fdf76d4bde71a |
| Source note | uspto-grants-2014_05 |