HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodine → 3-isobutyl-4,4,6,6-tetramethyl-4,6-dihydrofuro[3,4-d]thiazol-2(3H)-imine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodine | HCID 807 | — |
| Reactant | Isobutylamine | HCID 6558 | — |
| Reactant | 2,2,5,5-Tetramethyltetrahydro-3-ketofuran | HCID 138511 | — |
| Reactant | Potassium thiocyanate | HCID 516872 | — |
| Product | 3-isobutyl-4,4,6,6-tetramethyl-4,6-dihydrofuro[3,4-d]thiazol-2(3H)-imine | HCID 66851859 | — |
Reaction Steps
Commercially available 2,2,5,5-tetramethyldihydrofuran-3(2H)-one (Aldrich), 2-methylpropan-1-amine (Aldrich), potassium thiocyanate (Aldrich) and iodine (EMD chemicals) were processed using the method described in Example 17A to afford the title compound. MS (ESI+) m/z 255 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08735434B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-64aed7f52d7c4c0fbeef5d784980a02b |
| Source note | uspto-grants-2014_05 |