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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1028308Generated: October 31, 2026

Water → HCID 15886922, compound

https://huagongshe.com/reaction/1028308

Reaction equation

Participants

RoleNameHCIDCharge
ReactantWaterHCID 962—
ReactantN-bromobutanimideHCID 67184—
Reactant3-Methoxy-9H-carbazoleHCID 519621—
SolventDimethylformamideHCID 6228—
ProductHCID 15886922HCID 15886922—

Reaction Steps

3-Methoxy-9H-carbazole (Bedford, R. B.; Betham, M. J. Org. Chem. 2006, 71, 9403-9410) (0.029 g, 0.147 mmol) was dissolved in dry DMF (0.28 mL) and NBS (0.026 g, 0.147 mmol) was added to the solution. The reaction mixture was stirred at room temperature for 2 h under absence of light. The solution was poured into water (2 mL), filtered and washed with water. The title compound was isolated as a grey solid (0.033 g, 82%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08735440B2
Source datasetuspto-grants-2014_05
ORD IDord-4ea6780cbf744fd5a207b1f181300c46
Source noteuspto-grants-2014_05