Acetanilide → HCID 25216868, compound

Participants

Reaction Steps

The title compound was prepared with the analogous procedure described in example 3 using 4-Bromo-2-methyl-3-nitrobenzoic acid methyl ester and N-phenylacetamide (81 mg, 0.6 mmol) as starting materials to yield the title compound as yellow solid. 1H NMR (DMSO) δ 2.49 (s, 3 H), 2.62 (s, 3 H), 7.18 (d, J=8.6 Hz, 1 H), 7.28 (d, J=8.6 Hz, 1 H), 7.52-7.61 (m, 6 H); 13C NMR δ 13.5, 14.7, 51.8, 108.0, 123.7, 125.9, 126.9, 129.7, 130.1, 130.2, 134.0, 136.5, 138.0, 152.8, 167.2.

Provenance & Evidence