Acetanilide → HCID 23094067, compound

Participants

Reaction Steps

The title compound was prepared with the analogous procedure described in example 1 using 2,5-Dibromonitrobenzene (140 mg, 0.5 mmol) and N-phenylacetamide (81 mg, 0.6 mmol) as starting materials to yield the title compound as a yellow solid (87 mg, 61%). 1H NMR (DMSO) δ 2.52 (s, 3 H), 7.18 (d, J=8.8 Hz, 1 H), 7.43 (d, J=8.8 Hz, 1 H), 7.58-7.68 (m, 5 H), 7.98 (br s, 1 H); 13C NMR δ 13.5, 112.5, 115.5, 119.5, 126.4, 126.9, 129.6, 130.1, 134.0, 139.0, 154.2, 156.8.

Provenance & Evidence