HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylacetylene → HCID 58168095, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylacetylene | HCID 10821 | — |
| Reactant | 1-Chlorobenzo[C][1,8]naphthyridin-6(5H)-one | HCID 58168008 | — |
| Product | HCID 58168095 | HCID 58168095 | 68.3% |
Reaction Steps
The title compound was synthesized according to the procedure described for the preparation of Example 160 using Compound 83 (100 mg, 0.43 mmol) and ethynyl benzene (66 mg, 0.65 mmol) to provide 161 (87 mg, 67% yield) as a light-yellow solid. LC-MS (M+H=297, obsd.=297).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08735584B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-81c491728acd4f62867f7b51401eea50 |
| Source note | uspto-grants-2014_05 |