HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,5-Dichloro-nicotinoyl chloride → HCID 58168141, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,5-Dichloro-nicotinoyl chloride | HCID 2799996 | — |
| Reactant | HCID 58168352 | HCID 58168352 | — |
| Product | HCID 58168141 | HCID 58168141 | 48% |
Reaction Steps
The title compound was synthesized according to the procedure described for the preparation of Example 180 using Compound 185 (50 mg, 0.16 mmol) and 2,5-dichloro-nicotinoyl chloride (36 mg, 0.17 mmol) to provide 186 (37 mg, 48% yield) as a dark solid. LC-MS (M+H=496, obsd.=496).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08735584B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-9c39f8f96e2040c4badcd2bf72a9e10a |
| Source note | uspto-grants-2014_05 |