HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chloroaniline → HCID 58168201, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chloroaniline | HCID 7932 | — |
| Reactant | 1-Chlorobenzo[C][1,8]naphthyridin-6(5H)-one | HCID 58168008 | — |
| Product | HCID 58168201 | HCID 58168201 | 69.4% |
Reaction Steps
The title compound was synthesized according to the procedure described for the preparation of Example 188 using Compound 83 (100 mg, 0.43 mmol) and 3-chloroaniline (83 mg, 0.65 mmol) to provide 191 (96 mg, 68% yield) as a white solid. LC-MS (M+H=322, obsd.=322).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08735584B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-13e08128f035494d91ba3dcd41b98705 |
| Source note | uspto-grants-2014_05 |