HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chloroaniline → HCID 58168283, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chloroaniline | HCID 7812 | — |
| Reactant | 1-Chlorobenzo[C][1,8]naphthyridin-6(5H)-one | HCID 58168008 | — |
| Product | HCID 58168283 | HCID 58168283 | 98.3% |
Reaction Steps
The title compound was synthesized according to the procedure described for the preparation of Example 188 using Compound 83 (100 mg, 0.43 mmol) and 4-chloroaniline (83 mg, 0.65 mmol) to provide 192 (136 mg, 97% yield) as a white solid. LC-MS (M+H=322, obsd.=322).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08735584B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-af2a450ad2ce4c6892e7595830f1179a |
| Source note | uspto-grants-2014_05 |