HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,5-Dichloroaniline → HCID 58168213, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,5-Dichloroaniline | HCID 7262 | — |
| Reactant | 1-Chlorobenzo[C][1,8]naphthyridin-6(5H)-one | HCID 58168008 | — |
| Product | HCID 58168213 | HCID 58168213 | 32.6% |
Reaction Steps
The title compound was synthesized according to the procedure described for the preparation of Example 188 using Compound 83 (100 mg, 0.43 mmol) and 2,5-di-chloroaniline (105 mg, 0.65 mmol) to provide 199 (50 mg, 32% yield) as a white solid. LC-MS (M+H=356, obsd.=356).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08735584B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-b80322490bf440bc949379ec24b60dea |
| Source note | uspto-grants-2014_05 |