HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Chloro-2-methylaniline → HCID 58168359, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Chloro-2-methylaniline | HCID 7260 | — |
| Reactant | 1-Chlorobenzo[C][1,8]naphthyridin-6(5H)-one | HCID 58168008 | — |
| Product | HCID 58168359 | HCID 58168359 | 78.3% |
Reaction Steps
The title compound was synthesized according to the procedure described for the preparation of Example 188 using Compound 83 (100 mg, 0.43 mmol) and 5-chloro-2-methylaniline (80 mg, 0.56 mmol) to provide 206 (113 mg, 78% yield) as a white solid. LC-MS (M+H=336, obsd.=336).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08735584B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-fe8ed1242f7b4224b3f64c35433275a1 |
| Source note | uspto-grants-2014_05 |