p-Toluidine → HCID 58168258, compound

Participants

Reaction Steps

The title compound was synthesized according to the procedure described for the preparation of Example 231 using 6 (50 mg, 0.22 mmol) and p-toluidine (35 mg, 0.33 mmol) to provide 238 (14 mg, 21% yield) as a black solid. LC-MS (M+H=302, obsd.=302). 1H NMR (400 MHz, d6-DMSO): δ 11.64 (s, 1H), 8.82 (s, 1H), 8.44 (m, 2H), 8.12 (d, 1H), 7.78 (d, 1H), 7.27 (m, 1H), 7.22 (dd, 1H), 7.19 (s, 3H), 2.30 (s, 4H).

Provenance & Evidence