HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Fluoro-4-methylaniline → HCID 58168322, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Fluoro-4-methylaniline | HCID 9957 | — |
| Reactant | 9-chloro-5H-benzo[c][1,8]naphthyridin-6-one | HCID 58168298 | — |
| Product | HCID 58168322 | HCID 58168322 | 22.6% |
Reaction Steps
The title compound was synthesized according to the procedure described for the preparation of Example 231 using 6 (100 mg, 0.43 mmol) and 3-fluoro-4-methylaniline (0.07 mL, 0.65 mmol) to provide 246 (31 mg, 20% yield) as a brown solid. LC-MS (M+H (parent)=321, obsd.=321).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08735584B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-fbbdf11fd73040218244372494f6ca24 |
| Source note | uspto-grants-2014_05 |