Aniline → HCID 58168022, compound
Reaction equation
C([NH:8][C:9]([C:11]1[N:12]([CH3:32])[CH:13]=[C:14]([NH:16][C:17]2[CH:26]=[CH:25][N:24]=[C:23]3[C:18]=2[C:19]2[CH:31]=[CH:30][CH:29]=[CH:28][C:20]=2[C:21](=[O:27])[NH:22]3)[CH:15]=1)=[O:10])C1C=CC=CC=1.N[C:34]1[CH:39]=[CH:38][CH:37]=[CH:36][CH:35]=1>>[CH3:32][N:12]1[CH:13]=[C:14]([NH:16][C:17]2[CH:26]=[CH:25][N:24]=[C:23]3[C:18]=2[C:19]2[CH:31]=[CH:30][CH:29]=[CH:28][C:20]=2[C:21](=[O:27])[NH:22]3)[CH:15]=[C:11]1[C:9]([NH:8][C:34]1[CH:39]=[CH:38][CH:37]=[CH:36][CH:35]=1)=[O:10]Participants
3
Procedure
The title compound was synthesized according to the procedure described for the preparation of Example 300 using the carboxylic acid intermediate from example 310 and aniline to provide 312. LC-MS (M+H=410, obsd.=410).
Workup
- customThe title compound was synthesized
Sources & evidence
- ORD record
- ord-a5497c3a2bc64418b416aaf3e9747382
- Source dataset
- uspto-grants-2014_05
- Patent number
- US08735584B2
Reaction notes
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