Phenyl isocyanate → HCID 58168139, compound

HRID 1029257Notes

Reaction equation

HRID 1029257 reaction equation
[C:1]([N:9]1[CH2:12][CH:11]([NH:13][C:14]2[CH:23]=[CH:22][N:21]=[C:20]3[C:15]=2[C:16]2[CH:28]=[CH:27][CH:26]=[CH:25][C:17]=2[C:18](=[O:24])[NH:19]3)[CH2:10]1)(=[O:8])C1C=CC=CC=1.[N:29]([C:32]1[CH:37]=[CH:36][CH:35]=[CH:34][CH:33]=1)=C=O>>[O:24]=[C:18]1[C:17]2[CH:25]=[CH:26][CH:27]=[CH:28][C:16]=2[C:15]2[C:20](=[N:21][CH:22]=[CH:23][C:14]=2[NH:13][CH:11]2[CH2:10][N:9]([C:1]([NH:29][C:32]3[CH:37]=[CH:36][CH:35]=[CH:34][CH:33]=3)=[O:8])[CH2:12]2)[NH:19]1

Participants

3

Reactant 2

HCID 7672Phenyl isocyanateHCID 58168313HCID 58168313, compound

Product 1

HCID 58168139HCID 58168139, compound

Procedure

The title compound was synthesized according to the procedure described for the preparation of Example 359 using the amine intermediate from example 366 and isocyanato benzene to provide 367. LC-MS (M+H=386, obsd.=386).

Workup

  1. customThe title compound was synthesized

Sources & evidence

ORD record
ord-9b970fe8f13f4427ad5676d0c0a27be1
Source dataset
uspto-grants-2014_05
Patent number
US08735584B2

Reaction notes

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