2-Bromobenzyl bromide → HCID 44205296, compound

Participants

Reaction Steps

The title compound was synthesized according to the procedure described for the preparation of Example 458 using 70 (151 mg, 0.71 mmol) and 1-(bromo-methyl)-2-bromobenzene (214 mg, 0.86 mmol) to provide 469 (11 mg, 4% yield) as a white powder. LC-MS (M+H=381, obsd.=381). 1H NMR (400 MHz, DMSO-D6) δ 11.50 (m, 1H), 8.53 (m, 1H), 8.39 (m, 1H), 8.01 (d, J=8.9, 1H), 7.68 (s, 1H), 7.43 (m, 2H), 7.37 (s, 1H), 7.23 (s, 2H), 6.92 (m, 2H), 4.55 (s, 2H).

Provenance & Evidence