2-Pyridineethanamine → HCID 58167995, compound

Participants

Reaction Steps

The title compound was synthesized according to the procedure described for the preparation of Example 456 using 6 (162 mg, 0.70 mmol) and 2-(pyridin-2-yl)ethanamine (343 mg, 2.81 mmol) to provide 477 (10 mg, 5% yield) as a white powder. LC-MS (M+H=317, obsd.=317). 1H NMR (400 MHz, DMSO-D6) δ 11.52 (s, 1H), 8.73 (dd, J=6.6, 27.5, 2H), 8.44 (d, J=4.7, 1H), 8.15 (m, 1H), 8.00 (d, J=8.8, 1H), 7.63 (m, 2H), 7.19 (m, 2H), 6.97 (t, J=43.4, 1H), 3.71 (t, J=6.9, 2H), 3.25 (t, J=6.8, 2H).

Provenance & Evidence