HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetone → 5-n-Propyl-2,2-dimethyl-1,3-benzodioxol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | 4-Propyl-1,2-benzenediol | HCID 97638 | — |
| Reactant | p-Toluenesulfonic acid monohydrate | HCID 521998 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | 5-n-Propyl-2,2-dimethyl-1,3-benzodioxol | HCID 15165616 | — |
Reaction Steps
The same procedures as described in Example 10 were carried out by using a mixture of 7.61 g (50 mM) of 4-n-propylcatechol, 15 ml of acetone, 30 mg of p-toluenesulfonic acid monohydrate and 15 ml of benzene. 5-n-Propyl-2,2-dimethyl-1,3-benzodioxol was obtained in the yield of 9.13 g (47 mM) as colorless transparent liquid having a boiling point of 82°-87° C./3 mmHg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05102906 |
| Source dataset | uspto-grants-1992_04 |
| ORD ID | ord-7ec7997eb0bc4bd8a91d551f175836f3 |
| Source note | uspto-grants-1992_04 |