Acetyl chloride → HCID 14883529, compound
Reaction equation
[C:1]([NH:10][C@H:11]([C@H:14]([OH:20])/[CH:15]=[CH:16]/[CH2:17][CH2:18][CH3:19])[CH2:12][OH:13])(=[O:9])[CH2:2]CCCCCC.N[C@H]([C@H](O)/C=C/CCC)CO.C(Cl)(=O)C>>[C:1]([NH:10][C@H:11]([C@H:14]([OH:20])/[CH:15]=[CH:16]/[CH2:17][CH2:18][CH3:19])[CH2:12][OH:13])(=[O:9])[CH3:2]Participants
4
Procedure
Compound (7) is prepared analogously to the process described for (6) by using 117.9 mg (0.75 mMol) of compound (5) and 58.1 mg (0.74 mg) acetyl chloride.
Sources & evidence
- ORD record
- ord-eee43f69805947aebddb3eb7bf23a583
- Source dataset
- uspto-grants-1992_04
- Patent number
- US05103002
Reaction notes
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