Potassium Hydroxide → HCID 19901125, compound

HRID 1029791Notes

Reaction equation

HRID 1029791 reaction equation
[S:1]1[CH2:4][S:3][C:2]1=[C:5]([C:11]([O:13]CC)=[O:12])[C:6]([O:8][CH2:9][CH3:10])=[O:7].[OH-].[K+]>C(O)C>[S:1]1[CH2:4][S:3][C:2]1=[C:5]([C:11]([OH:13])=[O:12])[C:6]([O:8][CH2:9][CH3:10])=[O:7]

Participants

4

Reactant 2

HCID 14797Potassium HydroxideHCID 15565634Diethyl (1,3-dithietan-2-ylidene)propanedioate

Product 1

HCID 19901125HCID 19901125, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

Diethyl 2-(1,3-dithietan-2-ylidene)malonate was treated with a solution of potassium hydroxide in ethanol. The resultant solid was isolated and purified by the same method as in Example 1 to afford the titled compound as a white solid. (51%).

Workup

  1. customThe resultant solid was isolated
  2. custompurified by the same method as in Example 1

Sources & evidence

ORD record
ord-192d02d1cbd44f0e857d2f19aac69229
Source dataset
uspto-grants-1992_04
Patent number
US05103013

Reaction notes

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