HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → Isopropyl 2-(1,3-dithiolan-2-ylidene)-2-carboxyacetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | Isoprothiolane | HCID 39681 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | Isopropyl 2-(1,3-dithiolan-2-ylidene)-2-carboxyacetate | HCID 19901144 | — |
Reaction Steps
Diisopropyl 2-(1,3-dithiolan-2-ylidene)malonate was treated with a solution of potassium hydroxide in isopropyl alcohol. The resultant solid was isolated and purified by the same method as in Example 1 to afford the titled compound as a white solid. (64%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05103013 |
| Source dataset | uspto-grants-1992_04 |
| ORD ID | ord-0ed5ad2b78c74541b0ad936cbb789840 |
| Source note | uspto-grants-1992_04 |