2-Aminopyridine → HCID 19901133, compound

HRID 1029803Notes

Reaction equation

[S:1]1[CH2:4][S:3][C:2]1=[C:5]([C:11]([O:13]N1C2C=CC=CC=2N=N1)=O)[C:6]([O:8][CH2:9][CH3:10])=[O:7].[NH2:23][C:24]1[CH:29]=[CH:28][CH:27]=[CH:26][N:25]=1>>[S:3]1[CH2:4][S:1][C:2]1=[C:5]([C:11](=[O:13])[NH:23][C:24]1[CH:29]=[CH:28][CH:27]=[CH:26][N:25]=1)[C:6]([O:8][CH2:9][CH3:10])=[O:7]

Participants

Reactant 2

HCID 104392-Aminopyridine

HCID 19901137HCID 19901137, compound

Product 1

HCID 19901133HCID 19901133, compoundYield 51%

Procedure

Following the procedure of Example 27, the titled compound (51%) was prepared from ethyl 2-(1,3-dithietan-2-ylidene)-2-[(1-benzotriazolyl)oxycarbonyl]acetate and 2-aminopyridine.

Sources & evidence

ORD record: ord-d2dbb56f1cd7416396215738f7b953b7
Source dataset: uspto-grants-1992_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05103013

Reaction notes

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