HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylhydrazine → HCID 15754483, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylhydrazine | HCID 6061 | — |
| Reactant | Sulcotrione | HCID 91760 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 15754483 | HCID 15754483 | — |
Reaction Steps
2 g of 2-(2-chloro-4-methanesulfonylbenzoyl)cyclohexane-1,3-dione are dissolved in 50 ml of ethanol, 0.28 g of methylhydrazine are added, and the solution is then refluxed for 4 hours. It is subsequently allowed to cool, and the precipitate which has separated out is filtered off with suction. 0.85 g (41% of theory) of the desired product of the formula ##STR9## of melting point 208° C. is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05104442 |
| Source dataset | uspto-grants-1992_04 |
| ORD ID | ord-689f4ea0f0d74459a590ada62095c8fd |
| Source note | uspto-grants-1992_04 |