HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formaldehyde → HCID 54200907, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formaldehyde | HCID 712 | — |
| Reactant | HCID 13526351 | HCID 13526351 | — |
| Solvent | 1-Octanol | HCID 957 | — |
| Product | HCID 54200907 | HCID 54200907 | — |
Reaction Steps
The title compound was prepared from (S)-(-)-N-1-phenylethyl-N-trimethylsilylmethylamine by reaction with n-octanol and aqueous formaldehyde following the procedure of Example 2 to give the crude acetal (90% pure) as a colourless oil (9.1 g, 91%) δC (CD2Cl2)-1.28 (SiMe3), 14.29, 23.08, 30.31, 29.74, 29.89, 26.82, 33.32, 63.13 (O Octyl), 19.37 (CMe), 40.11 (NCH2Si), 62.10 (CH), 84.69 (NCH2O), 126.82, 127.96, 128.31, 145.95 (Ph).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05104989 |
| Source dataset | uspto-grants-1992_04 |
| ORD ID | ord-15da4e79ff444f1b95c0184e68ef402f |
| Source note | uspto-grants-1992_04 |