Magnesium ethanolate → HCID 86745678, compound

HRID 1030327Notes

Reaction equation

[Al:1].[O-:2][CH2:3][CH3:4].[Mg+2:5].[O-:6][CH2:7][CH3:8]>>[O-:2][CH2:3][CH3:4].[Mg+2:5].[O-:6][CH2:7][CH3:8].[CH3:4][CH:3]([CH3:7])[O-:2].[Al+3:1].[CH3:4][CH:3]([CH3:7])[O-:2].[CH3:4][CH:3]([CH3:7])[O-:2]

Participants

Reactant 2

HCID 164963Magnesium ethanolate

HCID 5359268Aluminum

Product 1

HCID 86745678HCID 86745678, compound

Procedure

One gram (5 mmoles) of aluminum ispropoxide was dissolved in 10 ml of Freon TF solvent and 0.7 grams (6 mmoles) of magnesium ethoxide added. After mixing in an ultra-sonic bath, followed by settling of suspended matter, 3 ml of the clear solution was analyzed for Mg and Al. Theory Al: 1.5 mmole, Found Al: 1.5 mmole. Theory Mg: 1.8 mmoles, Found Mg: 0.08 mmoles. Conclusion: Little effect of Aluminum alkoxide on solubility of Magnesium alkoxide in Freon TF, and therefore not a useful system for deacidification of books.

Workup

additionadded
additionAfter mixing in an ultra-sonic bath

Sources & evidence

ORD record: ord-c1e0fb6829274e59a977ac140224c39a
Source dataset: uspto-grants-1992_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05104997

Reaction notes

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