Ethylene Glycol → HCID 13781049, compound
Reaction equation
[C:1]([C:4]1[CH:11]=[CH:10][C:7]([CH2:8]Cl)=[C:6]([CH2:12][CH2:13][CH3:14])[C:5]=1[OH:15])(=[O:3])[CH3:2].[CH2:16]([OH:19])[CH2:17][OH:18]>>[C:1]([C:4]1[CH:11]=[CH:10][C:7]([CH2:8][O:18][CH2:17][CH2:16][OH:19])=[C:6]([CH2:12][CH2:13][CH3:14])[C:5]=1[OH:15])(=[O:3])[CH3:2]Participants
3
Procedure
Following the procedure of Example 48, 6.8 g. of 4-acetyl-3-hydroxy-2-propylbenzyl chloride and 150 ml. of ethylene glycol were reacted to provide 4.6 g. of the title alcohol. NMR.
Workup
- customto provide 4.6 g
Sources & evidence
- ORD record
- ord-1725ec6dab384785abff926ccb026d9d
- Source dataset
- uspto-grants-1992_04
- Patent number
- US05105017
Reaction notes
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