Sodium Hydroxide → HCID 19820014, compound

HRID 1030436Notes

Reaction equation

HRID 1030436 reaction equation
[N+:1]([C:4]1[CH:9]=[C:8]([CH3:10])[CH:7]=[CH:6][C:5]=1[I:11](Cl)Cl)([O-:3])=[O:2].[OH-:14].[Na+]>>[N+:1]([C:4]1[CH:9]=[C:8]([CH3:10])[CH:7]=[CH:6][C:5]=1[I:11]=[O:14])([O-:3])=[O:2]

Participants

3

Reactant 2

HCID 14798Sodium HydroxideHCID 85651777HCID 85651777, compound

Product 1

HCID 19820014HCID 19820014, compound

Procedure

2-Nitro-4-methyl(dichloroiodo)benzene (2.0 g, 6.0 mmol) was added portion-wise, over a period of 15 min, to a cold (5° C.), stirred solution of 20 percent aqueous sodium hydroxide (100 mL). Five min after the addition, the desired product, an orange solid, insoluble in the reaction medium, was isolated by filtration; yield, 1.51. g.

Workup

  1. additionFive min after the addition

Sources & evidence

ORD record
ord-999d3e55963c4452a60521bd1dc2878c
Source dataset
uspto-grants-1992_04
Patent number
US05106407

Reaction notes

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