Sodium Hydroxide → HCID 19820004, compound

HRID 1030437Notes

Reaction equation

HRID 1030437 reaction equation
[N+:1]([C:4]1[CH:9]=[C:8]([Cl:10])[CH:7]=[CH:6][C:5]=1[I:11](Cl)Cl)([O-:3])=[O:2].[OH-:14].[Na+]>>[N+:1]([C:4]1[CH:9]=[C:8]([Cl:10])[CH:7]=[CH:6][C:5]=1[I:11]=[O:14])([O-:3])=[O:2]

Participants

3

Reactant 2

HCID 14798Sodium HydroxideHCID 19820028HCID 19820028, compound

Product 1

HCID 19820004HCID 19820004, compound

Procedure

2-Nitro-4-chloro(dichloroiodo)benzene (2.0 g) was added to 100 mL of cold (about 5° C.) 20 percent aqueous solution of sodium hydroxide. The mixture was stirred for 0.5 hr, and the desired orange product was subsequently isolated by filtration and air dried; yield, 1.13 g; m.p. 118° C. (decomposed (dec.)).

Workup

  1. customthe desired orange product was subsequently isolated by filtration and air
  2. customdried
  3. customyield

Sources & evidence

ORD record
ord-7846bed897e34686904ef335487b5c2d
Source dataset
uspto-grants-1992_04
Patent number
US05106407

Reaction notes

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