HuagongsheHuagongshe Chemistry Print Report · For research reference only
Urea → HCID 15616398, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Urea | HCID 1176 | — |
| Reactant | 2-Naphthoic acid | HCID 7123 | — |
| Solvent | Thionyl Chloride | HCID 24386 | — |
| Product | HCID 15616398 | HCID 15616398 | 69.5% |
Reaction Steps
The above compound was prepared, following the procedure of Example 14a from 2-napthoic acid (8.2 g, 47.7 mmol), thionyl chloride (40 ml) and urea (10 g, 167 mmol) to give the title compound (7.1 g), mp 207°-208° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05106843 |
| Source dataset | uspto-grants-1992_04 |
| ORD ID | ord-e296b9aec77d4a9aa89fe0406df7476a |
| Source note | uspto-grants-1992_04 |