HCID 10446445, compound → HCID 9994098, compound

Participants

Reaction Conditions

Reaction Steps

N-[-1-cyano-1-(2-pyridinyl)ehtyl]-4-methoxy-benzamide (4.7 g, 0.0167 mole) was dissolved in 100 mL methanolic ammonia and treated with 1.5 g Raney nickel under 50 psi and warmed to 40° C. for 10 hours. The mixture was filtered and the supernate concentrated in vacuo to yield a pale green oil. The crude product (2.3 g) was used in the next step without further purification.

Provenance & Evidence