HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2'-Hydroxy-3'-isopentyl-4',6'-bis(methoxymethoxy)acetophenone → 4-(Methoxymethoxy)benzaldehyde
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2'-Hydroxy-3'-isopentyl-4',6'-bis(methoxymethoxy)acetophenone | HCID 16094531 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Produkt | 4-(Methoxymethoxy)benzaldehyde | HCID 250074 | 100,3% |
Reaktionsschritte
In 3 ml of methanol were dissolved 1.40 g of the 2'-hydroxy-4',6'-bis(methoxymethoxy)-3'-isopentylacetophenone obtained in Production Example 16 and 715 mg of the p-methoxymethoxybenzaldehyde obtained in Production Example 25, and a 50% ethanol solution of sodium hydroxide (4.0 g/8 ml) was added to the solution and the mixture was stirred at room temperature for 1 day to effect a reaction.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05106871 |
| Quelldatensatz | uspto-grants-1992_04 |
| ORD ID | ord-16e34e9971be4733bf7dc37251a1c365 |
| Quellennotiz | uspto-grants-1992_04 |