HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54338605, compound → 1-[2,4-Bis(methoxymethoxy)phenyl]-3-(4-methoxymethoxyphenyl)-1-propanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54338605 | HCID 54338605 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 1-[2,4-Bis(methoxymethoxy)phenyl]-3-(4-methoxymethoxyphenyl)-1-propanone | HCID 19744892 | — |
Reaction Steps
Then, a suspension of 2.52 g of 5% palladium/carbon in 50 ml of ethyl acetate was hydrogenated for 2 hours, and a solution of 5.11 g of 2',4,4'-tris(methoxymethoxy)chalcone in 50 ml of ethyl acetate was added to the suspension and hydrogenation was carried out. After the reaction, the palladium/carbon was removed by filtration and the filtrate was concentrated under a reduced pressure to obtain 1-[2,4-bis(methoxymethoxy)phenyl]-3-(4-methoxymethoxyphenyl)-1-propanone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05106871 |
| Source dataset | uspto-grants-1992_04 |
| ORD ID | ord-b83bb429686c41d5828f503d22c45b52 |
| Source note | uspto-grants-1992_04 |