HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzaldehyde → HCID 2825753, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzaldehyde | HCID 240 | — |
| Reactant | Penicillamine | HCID 5852 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 2825753 | HCID 2825753 | 94.7% |
Reaction Steps
A 250 mL flask was charged with 20 mL of water and 2.0 g (13.4 mmol) of D-penicillamine. To the resulting colorless solution was added 1.4 g (13.3 mmol) of benzaldehyde dropwise over 2 minutes. The resulting suspension was stirred vigorously for 30 minutes and allowed to stand at room temperature overnight. The solids thus obtained were collected by filtration to yield 3.0 g (12.6 mmol) of the title thiazolidine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05106992 |
| Source dataset | uspto-grants-1992_04 |
| ORD ID | ord-61022a3929554738b2fcd8c6775dd25e |
| Source note | uspto-grants-1992_04 |