HRID1030844

反应详情

EQUATION

反应方程式

HRID 1030844 的结构方程式

PROCEDURE

实验过程

57 Ml of tert-butylbenzene and 8.2 g of anhydrous aluminum chloride are added to the solution of 2-acetyl-5-bromo-6-methoxynaphthalene obtained as in example 1a), while keeping the temperature at -10° C. The reaction mixture is kept for 16 hours under stirring at room temperature and then it is worked as in example 1 obtaining 41.8 g of product with a yield equal to 85.3% calculated on the basis of the starting material 1-bromo-2-methoxynaphthalene.

WORKUP

后处理

  1. customobtained as in example 1a),
  2. customat -10° C